AAS152HAAS252H

Applied Chemistry for Soil, Water and Agro Systems Lab

L-T-P0-0-2 Credits1 Session2026-27 TypeLab / Practical
Appears in 2 semesters

B.Tech Agricultural Engineering · Sem 1 (Physics Lab / Chemistry Lab, code AAS152H) · B.Tech Agricultural Engineering · Sem 2 (Physics Lab / Chemistry Lab, code AAS252H)

List of Experiments / Activities

  1. 1Determination of Soil pH and Electrical Conductivity — Measure pH and electrical conductivity (EC) of soil samples (1:2.5 soil : water suspension) using pH meter and conductivity meter; interpret for agricultural suitability and salinity class
  2. 2Determination of Organic Carbon in Soil (Walkley-Black Method) — Determine organic carbon content in soil samples by wet oxidation using K2Cr2O7; titrate with ferrous ammonium sulphate (FAS); calculate % organic carbon and soil organic matter
  3. 3Estimation of Available Nitrogen — Estimate available nitrogen in soil by alkaline potassium permanganate in Soil (Alkaline KMnO4 Method) distillation method; titrate with standard H2SO4; calculate available N content; relate to nitrogen fertiliser recommendation
  4. 4Determination of Total Hardness of Irrigation Water — Determine total hardness (calcium and magnesium) of irrigation water by EDTA complexometric titration; relate to scaling in drip/sprinkler systems and soil sodicity
  5. 5Determination of Chloride in Water (Mohr's Method) — Estimate chloride content in irrigation water by argentometric titration; assess water quality for irrigating salt-sensitive crops; relate to Sodium Adsorption Ratio (SAR)
  6. 6Determination of COD and BOD of Agro-processing Wastewater — Determine COD of agro-industry wastewater (dairy/food processing effluent) by dichromate method; estimate BOD; relate to environmental impact and effluent treatment requirements
  7. 7Identification of Fertilisers by Chemical Tests — Identify given fertiliser samples (urea, ammonium sulphate, DAP, SSP, KCl) by systematic chemical tests (flame test, NH3 evolution, SO4²⁻ test, PO4³⁻ test); relate to fertiliser chemistry and nutrient content
  8. 8Estimation of Nitrogen in Fertiliser (Kjeldahl Method) — Determine nitrogen content of a fertiliser sample (urea or ammonium sulphate) by Kjeldahl digestion and distillation; titrate distillate; calculate % N; relate to fertiliser grade and quality certification
  9. 9Estimation of Crude Fat in Food Sample (Soxhlet Method) — Determine crude fat content in oilseeds or food samples (groundnut, soybean) by Soxhlet extraction using petroleum ether; calculate % fat.
  10. 10Detection of Food Adulterants — To identify common adulterants in milk, turmeric, and edible oils.
  11. 11Compost Quality Analysis – pH, C:N Ratio — Determine pH, electrical conductivity, and C:N ratio of compost and vermicompost samples; assess maturity and quality; relate to green fertiliser chemistry and soil health
  12. 12Green Synthesis of Biopesticide / Neem Extract Characterisation — Prepare aqueous neem leaf extract; determine pH, specific gravity, and azadirachtin qualitative test; compare with commercial formulation; relate to biopesticide chemistry and sustainable agriculture
Course Objectives5 points
  • To determine the chemical properties of soil including pH, organic matter, and nutrient content
  • To perform water quality analysis relevant to irrigation and agro-processing
  • To identify and characterise fertilisers and agrochemicals by chemical tests
  • To perform food quality analysis of agro-products
  • To apply green chemistry principles in sustainable agricultural systems
Course Outcomes (COs)5 outcomes

After completion of the course student will be able to:

  1. CO1Determine soil pH, organic carbon, and available nitrogen by standard analytical methodsK3
  2. CO2Analyse irrigation water quality for hardness, chloride, COD, and BODK3
  3. CO3Identify fertilisers by chemical tests and estimate nitrogen content by Kjeldahl methodK3
  4. CO4Determine fat and carbohydrate content of agro-products by extraction and colorimetric methodsK3
  5. CO5Evaluate compost quality and characterise green biopesticide preparationsK3

Suggested Textbooks / Reference Books

  1. Engineering Chemistry – Jain and Jain
  2. Soil Chemistry – Bohn, McNeal, and O'Connor
  3. Food Chemistry – Fennema (Ed.) Safety and General Instructions
  4. Students must wear lab coat and safety goggles at all times in the chemistry laboratory
  5. Handle all acids, alkalis, and oxidising agents with extreme care; use fume hood for volatile chemicals
  6. Dispose of chemical waste in designated containers as per lab safety guidelines
  7. Do not pipette by mouth; use rubber bulb or mechanical pipette fillers
  8. Wash hands thoroughly after every experiment; report any spillage or accident immediately

Official AKTU syllabus

This subject is on page 64, 65, 66, 67, 68 of the original AKTU PDF.

Official AKTU syllabus PDF ↗