List of Experiments / Activities
- Pharmaceutical Inorganic and Analytical Chemistry (Practical) Core Credit Hours Per Week (L-T-P) Max. Hours L T P
- 1-- --
- 45Maximum Marks SE ESE
- 1Limit tests (Any 4 Experiments) a. Limit test and modified limit test for Chloride as per Indian Pharmacopoeia b. Limit test and modified limit test for sulphate as per Indian Pharmacopoeia c. Limit test for Iron d. Limit test for Lead e. Limit test for arsenic
- 2Preparation of inorganic pharmaceuticals (Any 3 Experiments) a. Preparation of Aluminium hydroxide b. Preparation of potash alum c. Preparation of ferrous sulphate d. Preparation of Magnesium sulphate from magnesium hydroxide or magnesium carbonate
- 3Test for Purity (Any 2 Experiments) a. Assessment of swelling power of bentonite as per Indian Pharmacopoeia b. Evaluation of acid neutralizing capacity of aluminum hydroxide gel c. Determination of potassium iodate and iodine in potassium Iodide
- 4Assay of the following inorganic compounds including standardization of titrant (Any 5 Experiments) a. Assay of ammonium chloride by acid base titration, b. Assay of Ferrous sulphate by Cerimetry, c. Assay of Copper sulphate by Iodometry, d. Assay of Calcium gluconate by Complexometry, e. Assay of Hydrogen peroxide by Permanganometry, f. Assay of Sodium benzoate by non-aqueous titration, g. Assay of
Course Objectives
- The objectives of this course are to:
- Gain practical knowledge on various volumetric titration techniques.
- Learn the principles of volumetric analysis.
- Study the preparation and assessment of inorganic compounds.
- Determine the assay of various inorganic compounds in pharmaceutical use.
- Develop analytical skill for the qualitative and quantitative analysis of various inorganic compounds.
Course Outcomes (COs)
After completion of the course student will be able to:
- CO1Perform limit tests to detect and identify impurities in pharmaceutical substances.
- CO2Prepare various pharmaceutical inorganic compounds following standard procedures.
- CO3Analyze the significance of quality control in pharmaceutical products and raw materials.
- CO4Demonstrate proficiency in titrimetric analysis using different volumetric techniques.
- CO5Competence in applying analytical skills to qualitative and quantitative data.
Recommended References (Preferably Latest Editions):
- Bentley, R. and Driver, J., Chemistry. Oxford: Oxford University Press.
- Vogel, A.I., . Essex: Pearson Education Limited.
- Beckett, A.H. and Stenlake, J.B., Practical Pharmaceutical Chemistry. Part I & II. London: The Athlone Press, University of London.
- Kennedy, J.H., Analytical Chemistry: Principles. New York: Saunders College Publishing.
- Schroff, M.L., Inorganic Pharmaceutical Chemistry. New Delhi: Oxford Book Company.
- Indian Pharmacopoeia Commission, Indian Pharmacopoeia. Ghaziabad, India.
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